Scientific-Tecnical Services
Textural and Thermal Analysis Service
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Services
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External | |
---|---|---|
OPI / AGE / Universidades | Others | |
Differential Thermal Analysis and Thermogravimetry DTA-TG | 164,68 (€/sample) | 180,37 (€/sample) |
Differential Scanning Calorimetry (DSC) | 189,56 (€/sample) | 207,61 (€/sample) |
Contact
maqueda@icmse.csic.es
954 48 95 48
Physisorption-Chemisorption
This service constitutes a basic tool for the microstructural characterization of powdered solids of different natures, regarding to their porosity, specific surface area and chemically active surface.
This service is composed by a phyisisorption analyser (Micromeritics, ASAP 2020) which pro-vides the complete adsorption/desorption isotherms, from which the specific surface area, pore and micropore size distribution and concentration of reactive sites are obtained. The instrument is also equipped for carrying out chemisorption of different reactive molecules, as O2, H2, CO, etc.
Available Equipment
- Physicorption Analyser ASAP2010 (Micromeritics)
- Chemisorption Analyser ASAP2010 (Micromeritics)
- Multisample Physisorption Analyser TRISTAR II (Micromeritics)
- Multisample Physisorption Analyser TRISTAR II-Kr (Micromeritics)
Services
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External | |
---|---|---|
OPI / AGE / Universidades | Others | |
Temperature Programmed Desorption (TPD) | 79,55 (€/sample) | 87,13 (€/sample) |
Temperature Programmed Oxidation (TPO) | 79,55 (€/sample) | 87,13 (€/sample) |
Chemisorption | 79,55 (€/sample) | 87,13 (€/sample) |
Temperature Programmed Reduction (TPR) | 79,55 (€/sample) | 87,13 (€/sample) |
Specific Surface Area (BET) | 81,90 (€/sample) | 89,70 (€/sample) |
Superficie específica (Isoterma Adsorción-Desorción) | 90,11 (€/sample) | 98,69 (€/sample) |
Contact
gcolon@icmse.csic.es, caballero@us.es
954 48 95 36 - 954 48 95 43
Atomic Emission Spectrometry
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Services
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External | |
---|---|---|
OPI / AGE / Universidades | Others | |
Analysis of elements: ICP-OES. Análisis Elemental ICP-OES Muestras Líquidas | 20,60 (€/element) | 22,56 (€/element) |
Digestión de Muestra | 34,82 (€/sample) | 38,14 (€/sample) |
Contact
belinda@icmse.csic.es
954 48 95 39, int: 446139
Vibrational Spectroscopy Service
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Services
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External | |
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OPI / AGE / Universidades | Others | |
Spectroscopy: FT-IR
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67,61 (€/hour)
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74,05 (€/hour)
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Contact
mauricio.calvo@icmse.csic.es, centeno@icmse.csic.es
954 48 95 39
Micro-Raman Spectroscopy
Raman spectroscopy is based on a photonic process in which the incident radiation is dis-persed by the sample. This latter is perturbed leading to vibrational and rotational transitions. In general, the Raman spectrum is interpreted like a vibrational one, providing information very similar to the infrared spectroscopy, although the Raman active vibrations are not always the same as those excited with infrared radiation. A Raman vibration mode is active if there is a change of polarizability of the chemical bonds or the considered molecule, which in turn results in the generation of induced dipolar momentam. Its application fields are very broad: semiconductors, carbon compounds (graphite, diamond, nanotubes, fibers…), catalysts, pigments, etc.
Available Equipment
- LabRAM Horiba Jobin Yvon equipped with a confocal microscope and 3 excitation lasers (785 nm red, 532 nm green, and 325 nm UV)
Services
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External | |
---|---|---|
OPI / AGE / Universidades | Others | |
Micro-Raman Spectroscopy
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50,82 (€/hour)
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55,66 (€/hour)
|
Contact
centeno@icmse.csic.es, mauricio.calvo@icmse.csic.es
954 48 95 43 - 954 48 95 81 - 954 48 95 79
Electroluminescence Spectroscopy
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Services
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External | |
---|---|---|
OPI / AGE / Universidades | Others | |
Spectrophotometry and Photoluminescence | 147,64 (€/hour) | 161,71 (€/hour) |
Contact
mauricio.calvo@icmse.csic.es, h.miguez@csic.es
Ultraviolet-Visible-Near Infrared Spectroscopies
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Services
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External | |
---|---|---|
OPI / AGE / Universidades | Others | |
Spectroscopy: UV-Visible Spectral Reflectometry (CARY 300)
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19,75 (€/hour)
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21,64 (€/hour)
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Spectroscopy: UV-Visible Spectral Reflectometry-NIR (CARY 7000) |
34,95 (€/hour)
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38,28 (€/hour)
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Contact
glozano@icmse.csic.es, h.miguez@csic.es
954 48 95 39
Ultrafast Emission and Absorption Spectroscopy
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Services
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External | |
---|---|---|
OPI / AGE / Universidades | Others | |
Ultrafast Emission and Absorption Spectroscopy | 117,20 (€/hour) | 128,37 (€/hour) |
Contact
h.miguez@csic.es, juan.galisteo@csic.es
954 48 95 87
Chemical Surface Analysis by Electron Photoemission Service
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Services
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External | |
---|---|---|
OPI / AGE / Universidades | Others | |
Spectroscopy Ultraviolet Photoelectron Spectroscopy (UPS). Análisi de UPS o REELS o ISS con Técnico
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138,58 (€/hour)
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151,77 (€/hour)
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Spectroscopy X-ray Photoelectron Spectroscopy (XPS). Análisis XPS con Técnico
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103,28 (€/hour)
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113,12 (€/hour)
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Spectroscopy X-ray Photoelectron Spectroscopy (XPS). Tratamiento in situ con Técnico | 103,28 (€/hour) | 113,12 (€/hour) |
Spectroscopy X-ray Photoelectron Spectroscopy (XPS). Análisis Cuantitativo de los Datos con Técnico | 118,67 (€/hour) | 129,97 (€/hour) |
Spectroscopy X-ray Photoelectron Spectroscopy (XPS). Emisión de Informe Científico | 163,11 (€/hour) | 178,64 (€/hour) |
Contact
jpespinos@icmse.csic.es, holgado@icmse.csic.es
954 48 95 31 - 954 48 95 36
Surface Wetting Analysis
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Services
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External | |
---|---|---|
OPI / AGE / Universidades | Others | |
Determinación de Ángulo de Contacto en Superficie (Wetting Tension)
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55,80 (€/hour)
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61,11 (€/hour)
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Determinación de Ángulo de Contacto en Superficie (Wetting Ambiente Controlado)
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106,97 (€/hour)
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106,97 (€/hour)
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Determinación de Ángulo de Contacto en Superficie (Electrowetting)
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57,53 (€/hour)
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63,04 (€/hour)
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Determinación de Ángulo de Contacto en Superficie (Wetting - Informe)
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64,42 (€/hour)
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70,56 (€/hour)
|
Contact
mclopez@icmse.csic.es
Tribological and Mechanical Surface Characterization Service
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Services
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External | |
---|---|---|
OPI / AGE / Universidades | Others | |
Mechanical Properties of Materials at Microscale
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60,09 (€/hour)
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65,81 (€/hour)
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3D-Optical Microscopy Confocal/High Resolution Perfilometry/Interferometry
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75,50 (€/hour)
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82,69 (€/hour)
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Contact
jcslopez@icmse.csic.es
X-Ray Diffraction Laboratory
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Services
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External | |
---|---|---|
OPI / AGE / Universidades | Others | |
X-ray Scattering: Thin Film Characterization (Reflectivity, Reciprocal Space Maps) (Reflectometría de Rayos X) | 21,55 (€/hour) | 34,89 (€/hour) |
X-ray Scattering: Thin Film Characterization (Reflectivity, Reciprocal Space Maps) (Textura Empyrean) | 235,80 (€/hour) | 258,25 (€/hour) |
Structural Characterization: Qualitative X-ray powder diffraction analysis (Cargador) | 18,12 (€/hour) | 29,34 (€/hour) |
Structural Characterization: Qualitative X-ray powder diffraction analysis (Temperatura) | 19,29 (€/hour) | 31,22 (€/hour) |
Structural Characterization: Qualitative X-ray powder diffraction analysis (Kalfa1) | 80,27 (€/hour) | 87,92 (€/hour) |
Structural Characterization: Qualitative X-ray powder diffraction analysis (Microdifracción) | 84,89 (€/hour) | 92,97 (€/hour) |
Small Angle X Ray Scattering (SAXS) | 17,39 (€/hour) | 28,15 (€/hour) |
XRD (X-Ray Diffraction) of thin films (Panalytical) | 16,93 (€/hour) | 27,42 (€/hour) |
(X-Ray Diffraction) of thin films (Empyrean) | 149,19 (€/hour) | 163,39 (€/hour) |
Contact
creal@icmse.csic.es
954 13 92 17 (ext. 446123)
Electron Microscopy Service
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Services
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External | |
---|---|---|
OPI / AGE / Universidades | Others | |
Metal Coater (Sputtering)
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59,36 (€/10 samples)
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65,01 (€/10 samples)
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Scanning Electron Microscopy (SEM): High Resolution SEM
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57,33 (€/hour)
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70,98 (€/hour)
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Scanning Electron Microscopy (SEM): Low Voltage SEM
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57,33 (€/hour)
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70,98 (€/hour)
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Scanning Electron Microscopy (SEM): EDS(Energy Dispersive X-Rays Spectroscopy)
|
57,33 (€/hour)
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70,98 (€/hour)
|
Contact
tcrojas@icmse.csic.es, asuncion@icmse.csic.es, cjimenez@icmse.csic.es
Transmission Electron Microscopy
The transmission electron microscopy is a widely used technique for the microstructural and chemical characterization at micro and nanoscales, providing two-dimensional images of the sample texture and shape as well as grain and/or particle size, degree of homogeneity at the microscopic scale, degree of crystallinity of the sample, identification of crystalline phases, and high resolution images to identify the crystalline domains. The microscope is equipped with an EDX analyzer for compositional analysis. It can be applied to all type of materials and research topics in materials science and technology working with electron-transparent samples prepared ad-hoc for this end. The service performs transmission electron microscopy: Imaging in bright and dark field, selected area electron diffraction and high resolution electron microscopy, as well as elemental analysis of selected areas. It does not provide STEM mode.
Available Equipment
- JEOL 2100Plus microscope (200kV) with LaB6 filament. Structural resolution of 0.14 nm between lines and 0.23 nm between points. Sample holders with one and two angles. An X-ray Energy Dispersive Analyzer (EDX X-Max 80T, Oxford Instruments) and a CCD camera (Gatan) for image registration are attached to the equipment.
- Additional equipment in the “electron microscopy samples preparation laboratory”
Services
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External | |
---|---|---|
OPI / AGE / Universidades | Others | |
Structural Characterization: Tranmision Electron Microscopy (TEM)
|
88,06 (€/hour)
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96,45 (€/hour)
|
TEM: EDS (Energy Dispersive X-Rays Spectroscopy)
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88,06 (€/hour)
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96,45 (€/hour)
|
TEM: High Resolution TEM
|
88,06 (€/hour)
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96,45 (€/hour)
|
Contact
tcrojas@icmse.csic.es, asuncion@icmse.csic.es, olga@ciccartuja.es
Laboratory for Nanoscopies and Spectroscopies-LANE
The LANE laboratory has a TEM field emission microscope Tecnai F30, equipped with STEM mode, EDX and HAADF detectors, and an energy filter analyzer (GIF). In addition sample preparation equipment is available including plasma cleaning, surface polishing and thin films fabrication. The techniques available include: bright and dark field TEM; high resolution TEM; electron diffraction; STEM-HAADF analysis; EDX and STEM-EDX as well as EELS and STEM-EELS analysis (including point and line measurements and compositional maps); EFTEM images; spectrum-image and electron tomography analysis. More details about the LANE laboratory can be found on the website http://www.lane.icmse.csic.es/ (under construction).These facilities offer microstructural and chemical characterization especially devoted to the areas of materials science and physical chemistry of the solid state. It is relevant the high resolution analytical microscopy to characterize materials in the nano-scale..
Available Equipment
- Microscopio Tecnai G2 F30 S-TWIN 300KV con pistola de emisión de campo. Resolución estructural de 0,2 nm entre puntos, portamuestras de uno y dos ángulos. Adjuntos al equipo hay un detector de derivación de silicio EDX X-Max 80T Detector (Oxford Instruments) y un filtro de energía Gatan (GIF Quantum SE)
Services
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External | |
---|---|---|
OPI / AGE / Universidades | Others | |
Structural Characterization: Tranmision Electron Microscopy (TEM) |
121,12 (€/hour)
|
132,65 (€/hour)
|
TEM: EDS (Energy Dispersive X-Rays Spectroscopy)
|
121,12 (€/hour)
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132,65 (€/hour)
|
TEM: EELS (Electron Energy Loss Spectroscopy)
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121,12 (€/hour)
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132,65 (€/hour)
|
TEM: EFTEM (Energy Filtering TEM)
|
121,12 (€/hour)
|
132,65 (€/hour)
|
TEM: ELNES ( Energy-Loss Near-Edge Structures)
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121,12 (€/hour)
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132,65 (€/hour)
|
TEM: Spectrum imaging
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121,12 (€/hour) |
132,65 (€/hour)
|
TEM/STEM electron tomography
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121,12 (€/hour) |
132,65 (€/hour)
|
TEM: High Resolution TEM | 121,12 (€/hour) | 132,65 (€/hour) |
TEM: STEM/ADF-HAADF | 121,12 (€/hour) | 132,65 (€/hour) |
Contact
tcrojas@icmse.csic.es, asuncion@icmse.csic.es
Electron Microscopy Samples Preparation Laboratory
The laboratory for TEM and SEM samples preparation has a gold coater, a carbon evaporator, a metallization system for Cr and carbon, a diamond wheel cutter, a grinder with disc-grinder device, an ultrasonic cutter, a concave polishing (dimple) and ion thinning (Fischione 1010).
Services
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External | |
---|---|---|
OPI / AGE / Universidades | Others | |
Metalización (Sputtering)
|
59,36 (€/sample)
|
65,01 (€/sample)
|
Preparación de Láminas Delgadas y Probetas Delgado-Pulidas (Sección Transversal)
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212,81 (€/sample)
|
233,08 (€/sample)
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Preparación de Láminas Delgadas y Probetas Delgado-Pulidas (Visión Planar)
|
181,22 (€/sample)
|
198,48 (€/sample)
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Preparación de Láminas Delgadas y Probetas Delgado-Pulidas (Adelgazamiento Iónico)
|
29,79 (€/sample)
|
42,56 (€/sample)
|
Contact
tcrojas@icmse.csic.es, asuncion@icmse.csic.es
Preparation and characterization services of heterogeneous catalytic systems
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Services
|
External | |
---|---|---|
OPI / AGE / Universidades | Others | |
Evaluation of catalytic performance
|
86,51 (€/hour)
|
94,75 (€/hour)
|
Sample Preparation
|
86,51 (€/hour)
|
94,75 (€/hour)
|
Thermal and chemical treatments | 86,51 (€/hour) | 94,75 (€/hour) |
Contact
alfonso.caballero@csic.es
Mechanized Workshop
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Services
|
External | |
---|---|---|
OPI / AGE / Universidades | Others | |
CAD design of 2D or 3D parts | 1,84 (€/hour) | 2,01 (€/hour) |
Manufacturing of Parts by Removal Processes (Prototype Manufacturing) | on request | on request |
Manufacturing of Parts by Removal Processes (Machining with Lathe or Milling Machine) | 32,43 (€/hour) | 35,52 (€/hour) |
Rapid Prototyping of Parts by Plastic Deposition (Design and Manufacture of Plastic Parts 3D Printing) | 11,07 (€/hour) | 12,12 (€/hour) |
Contact
jcarlos.martin@csic.es
954 48 96 17 (ext. 446102)
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